Ultra Start 4500 Manuale delle Istruzioni

-EASUREWHATISMEASURABLEANDMAKEMEASURABLETHATWHICHISNOT'ALILEO'ALILEIInstruction ManualDMA 4500/5000Density/Specific G

3 Symbols in the Instruction Manual10 XDLIB073 Symbols in the Instruction ManualThe following symbols are used in the instruction manual:Warning:The &

Appendix C: Commands for Communication between PC and DMA 4500/5000100 XDLIB07get raw data ↵ actual Q, actual temperature, set temperature, sample ide

Appendix C: Commands for Communication between PC and DMA 4500/5000XDLIB07 101continue xx.xx ↵ measurement not startedmeasurement not finishedmeasurem

Appendix D: Density Tables102 XDLIB07Appendix D: Density TablesDensity of Dry AirAt the temperature t in [°C] and the pressure p in [mbar] or [hPa] th

Appendix D: Density TablesXDLIB07 103Density of Dry Air (-10°C to +90°C)3Composition of dry air in [v/v]: 78.110% N2; 20.938% O2; 0.916% Ar; 0.033% C

Appendix D: Density Tables104 XDLIB07Density of Water (0°C to 100°C)44. Literature: Spieweck, F. & Bettin, H.: Review: Solid and liquid density de

Appendix D: Density TablesXDLIB07 10536.993681 .993646 .993610 .993575 .993540 .993504 .993468 .993433 .993397 .99336137.993325 .993289 .993253 .99321

Appendix D: Density Tables106 XDLIB0777.973632 .973571 .973510 .973449 .973388 .973327 .973266 .973205 .973144 .97308378.973021 .972960 .972899 .97283

Appendix E: Possible Adjustment Errors, Adjustment ReportXDLIB07 107Appendix E: Possible Adjustment Errors, Adjustment ReportCause CorrectionDirect su

Appendix E: Possible Adjustment Errors, Adjustment Report108 XDLIB07Examples and explanations of KB-value deviations:Built-up deposits inside the U-tu

Appendix E: Possible Adjustment Errors, Adjustment ReportXDLIB07 109Adjustment Report Serial number of

4 Supplied ItemsXDLIB07 114 Supplied ItemsHints:• The DMA 4500/5000 has been tested and packed carefully before shipment. However, damage may occur du

Appendix F: Software Versions110 XDLIB07Appendix F: Software VersionsSoftware versionDate ofreleaseDocumentnumberCommentsV 2.004.b 30.03.1998 XDLIB07A

Appendix F: Software VersionsXDLIB07 111V 5.003.b 03.09.2003 XDLIB07J • "density" replaces the previous densities "density (viscosity &

Appendix G: Wetted Parts112 XDLIB07Appendix G: Wetted PartsThe following materials are in contact with the samples to be measured and with the cleanin

Appendix H: Menu TreeXDLIB07 113Appendix H: Menu TreeMenutemperature settingadjustset temperature °C, °Fadjustview adjustment dataprint adjustment dat

Appendix H: Menu Tree114 XDLIB07computer interface configurationdate & timelanguageexternal keyboard typechange password 4)english, Deutschtypenew

Appendix H: Menu TreeXDLIB07 115sample changer parameter 6)user functionssingle, doubleoutput configurationpolynomials 0 (2D), ...,polynomials 9 (2D)a

Appendix H: Menu Tree116 XDLIB07user tableshigh/low limitslow limit, high limitdata memorybrowserclear tableprint table datadata diagramactual Q, ...,

IndexXDLIB07 117IndexSymbols, (comma 55; (semicolon) 55<CR><LF> 55AAcid/base tables 63Adjustment 16, 28, 30, 47, 69, 108Adjustment coeffic

Index118 XDLIB07IUPAC 62KKAEMPF 62KB-value 49, 108Keyboard 45, 56Keyboard interface 97Keypad 44LLanguage 21, 56Line delimiter 54, 55, 96, 97Log file 8

IndexXDLIB07 119Testmode 76True density 37UUser formula 60, 68, 70User privileges 91User settings 46, 91User table 61, 68, 73U-tube 7, 58, 59, 108VVis

4 Supplied Items12 XDLIB072 Injection adapter LuerCat.No. 122252 Male Luer plug PTFECat.No. 638652 Adapter Luer coneCat.No. 638631 ScrewdriverCat.No.

5 Putting into OperationXDLIB07 135 Putting into OperationPreparing the DMA 4500/5000 for the first start-up1. Take 2# injection adapters Luer from th

5 Putting into Operation14 XDLIB074. Insert the screws (3) into the bore holes of the adapters and tighten the screws until some resistance against fu

5 Putting into OperationXDLIB07 159. If a printer will be used, plug the interface cable into the COM 2 connector at the rear of the DMA 4500/5000.10.

5 Putting into Operation16 XDLIB07Fig. 5 - 4 Placing of the waste vessel17. Open one bottle of the supplied liquid density standards (ultra pure water

6 Functional ComponentsXDLIB07 176 Functional Components6.1 Display and KeypadAfter turning on the DMA 4500/5000, the instrument carries out a self-te

6 Functional Components18 XDLIB07a) Date and timeb) Density with automatic viscosity correctionc) Specific gravity with automatic viscosityd) Measurin

6 Functional ComponentsXDLIB07 196.2 Front ViewFig. 6 - 2 Front view and keypadA LC displayB Inspection window for the measuring cellC Soft keysD &quo

6 Functional Components20 XDLIB076.3 Rear ViewFig. 6 - 3 Rear viewA "DRY AIR PUMP" nozzle for connecting a desiccator (see appendix A)B &quo

7 General SettingsXDLIB07 217 General Settings7.1 Display Contrast• Make sure that the instrument is set to the measuring mode.• The display contrast

7 General Settings22 XDLIB077.5 Setting the TemperatureSet the temperature to degrees Celsius or Fahrenheit in "temperature setting" (see ch

7 General SettingsXDLIB07 237.7 Defining the Display Contents and Layout• Select the items to be displayed and their size in "method settings&quo

7 General Settings24 XDLIB07• To list the selected items in your preferred order, highlight an item and move it up or down using the "Mov Up"

7 General SettingsXDLIB07 25•Use "↵" to toggle between "Y" (yes, selected) and "N" (no, not selected). Example for the &

7 General Settings26 XDLIB07• Select "sample changer configuration", "edit SHx/SCx mode" to enter the filling and cleaning paramet

7 General SettingsXDLIB07 27DMA 4500/5000:• Sample filling mode: This parameter is only displayed, if a sample changer/sample handling unit is connec

8 Checking Procedure, Adjustment and Calibration28 XDLIB078 Checking Procedure, Adjustment and Calibration8.1 DefinitionsAdjustment of the density met

8 Checking Procedure, Adjustment and CalibrationXDLIB07 29Fig. 8 - 1 Screen: Density check settings2. Make the settings corresponding to the density-c

Instruction ManualDMA 4500/5000Density/Specific Gravity/Concentration MeterSoftware Version: V5.012.c

8 Checking Procedure, Adjustment and Calibration30 XDLIB078.3 Adjustment• An adjustment has to be performed if deviations between the displayed values

8 Checking Procedure, Adjustment and CalibrationXDLIB07 315. Wait until the air adjustment is finished.6. Note down the current Q value of air in the

8 Checking Procedure, Adjustment and Calibration32 XDLIB07• By selecting "REPEAT" after "recommendation: REPEAT" is displayed, the

8 Checking Procedure, Adjustment and CalibrationXDLIB07 336. The temperature of the measuring cell ("set temperature") is automatically set

8 Checking Procedure, Adjustment and Calibration34 XDLIB078.3.3 Special Adjustment • Special adjustments are user-specific adjustments for special den

8 Checking Procedure, Adjustment and CalibrationXDLIB07 35Special adjustment procedure:1. The special adjustment is performed at the current set tempe

8 Checking Procedure, Adjustment and Calibration36 XDLIB078.4 Calibration• Calibrations are checking procedures which are carried out using certified

9 MeasurementsXDLIB07 379 Measurements1. Activate the required method using the "Method" soft key.• A method consists of the measuring tempe

9 Measurements38 XDLIB072. Ensure that the measuring cell is clean and dry.3. Fill the sample into the measuring cell.- OIML w/w: Measurement of ethan

9 MeasurementsXDLIB07 39There are several options for filling the samples into the measuring cell:A. By syringe with Luer tip, see Fig. 9 - 2.Fig. 9 -

While every precaution has been taken in the preparation of this document, Anton Paar GmbH assumes no responsibility for technical or printing errors

9 Measurements40 XDLIB07B. By gravity, using a funnel and a hose at the inlet and a hose with a valve (e.g. a clamp to block the flexible hose) at the

9 MeasurementsXDLIB07 41Press soft key "Sample#" to define a sample name and/or sample number. Measuring results are printed and stored auto

10 Cleaning and Drying the Measuring Cell42 XDLIB0710 Cleaning and Drying the Measuring Cell1. Fill the measuring cell with cleaning liquid 1 using a

10 Cleaning and Drying the Measuring CellXDLIB07 438. Turn off the air pump.9. Remove the air hose from the injection adapter Luer.

11 Operation44 XDLIB0711 Operation11.1 Menu OperationFig. 11 - 1 Main menu, audit trail function deactivated11.1.1 Using the Keys on the Keypad• To se

11 OperationXDLIB07 4511.1.2 Using an External Keyboard (Optional)• Connect a standard PC keyboard to the keyboard connector (PC/AT interface) at the

11 Operation46 XDLIB0711.2.3 "temperature setting"Any temperature from 0 to 90°C or 32 to 194°F can be set.→ export audit trail The log file

11 OperationXDLIB07 4711.2.4 "adjustment"→ adjust→ density (air, water) Adjustment at 20°C using air and water, detailed description see cha

11 Operation48 XDLIB07→ density The density coefficients used for calculating the density from the period of oscillation are displayed.→ KA: Density c

11 OperationXDLIB07 49→ deviation KB• Graphically displays the offsets of the KB-values with reference to the first KB-value displayed. The deviation

XDLIB07 5Contents1 Introduction...

11 Operation50 XDLIB0711.2.5 "measurement settings"Fig. 11 - 2 Screen: Measurement settings→ density check→ check density This function is u

11 OperationXDLIB07 51→ sample changer Automatic sample filling by sample changer/handling unit. If a sample changer is used the "Start" sof

11 Operation52 XDLIB07→ text The sample identification for printout, display and storage in the data memory is the text entered via the "Sample#&

11 OperationXDLIB07 53→ temperature scan: (only DMA 5000)This function can be used to increase or decrease the measuring temperature automatically in

11 Operation54 XDLIB0711.2.6 "instrument settings"→ display illumination→ switch off time: Screen saving mode (display illumination switches

11 OperationXDLIB07 55→ 2400→ 4800→ 9600→ computer interfaceconfigurationIf the DMA 4500/5000 is connected to a PC via COM1, the computer interface ha

11 Operation56 XDLIB07→ month→ day→ hour→ minute→ second→ format→ date format:→ dd.mm.yyyy→ mm/dd/yyyy→ yyyy-mm-dd→ weekday:→ yes→ no→ name of month:

11 OperationXDLIB07 5711.2.7 "method settings"Fig. 11 - 3 Screen: Method settings→output selection• From each listed menu you can select the

11 Operation58 XDLIB07→ method Method name for display, printout and memory.→ serial number Serial number for display and printout.→ sample number Sam

11 OperationXDLIB07 59→ Q Final quotient of the period of oscillation of the U-tube divided by the period of oscillation of the reference oscillator w

6 XDLIB0711.2.3 "temperature setting"... 4611.2.4

11 Operation60 XDLIB07→ App. density brass Apparent density referring to scales, which are adjusted with brass weights.Apparent density results are re

11 OperationXDLIB07 61→ user table 0 User-specified table converting density to concentration or any other related value.→ user table 1→ user table 2→

11 Operation62 XDLIB07→ IUPAC (%v/v) Alcohol concentration in percentage by volume according to the International Union of Pure and Applied Chemistry,

11 OperationXDLIB07 63→ extract/sugar tables 2 tables for the determination of saccharose/extract concentration of sugar in water using density are av

11 Operation64 XDLIB07→ nitric acid (HNO3)(%w/w)Aqueous nitric acid concentration in percentage by weight according to Landolt-Boernstein, based on tr

11 OperationXDLIB07 65→ dens. API 15°C-F(fuel, heating oil)Conversion of fuel density at measuring temperature to density at 15°C. → dens. API 60°F-F(

11 Operation66 XDLIB07→ reset output selection Resets the complete output selection to the factory default setting. Display, printer and memory settin

11 OperationXDLIB07 6711.2.8 "sample changer configuration"• This menu is only available if a sample changer/handling unit is connected.• If

11 Operation68 XDLIB0711.2.9 "user functions"• 1 user-specified formula, 3 user-specified tables, 5 user-specified polynomial equations and

11 OperationXDLIB07 69→ adjust Adjustment at "set temperature", using two density standards of your choice. For adjustment to special densit

1 IntroductionXDLIB07 71 IntroductionThank you for buying the DMA 4500 or DMA 5000 density/specific gravity/concentration meter for gases and liquids.

11 Operation70 XDLIB07→ trailing digits: Maximum of 6 digits after the decimal point.→ exponential: Enable or disable exponential format.→ sign: En

11 OperationXDLIB07 71→ second input selection The second input value for the user formula can be selected from the displayed list.→ output configurat

11 Operation72 XDLIB07→ input selection For each polynomial an individual input can be selected from the displayed listing. The most common input is d

11 OperationXDLIB07 73→ data diagram Graphically displays the polynomial function within two input values (e.g. density).→ min. value: Lower input val

11 Operation74 XDLIB07→ clear table Deletes all table values, name and settings.→ edit table data The table data are entered in data pairs. A maximum

11 OperationXDLIB07 7511.2.10 "custom function verification"• The DMA 4500/5000 can be used to calculate concentrations and other density re

11 Operation76 XDLIB0711.2.12 External CellThe external cell DMA HP (or the former models DMA 512 or DMA 602) can be connected to the DMA 4500/5000. F

11 OperationXDLIB07 7711.3 "Sample#"According to the settings in "measurement settings", "type of sample identif.", this

11 Operation78 XDLIB07• For sample identification by "list by number", a list of up to 60 individually selected numbers or texts can be ente

11 OperationXDLIB07 79Automatic activation:The appropriate measuring temperature for each sample can be pre-defined in the sample identification using

2 Safety Instructions8 XDLIB072 Safety Instructions• This instruction manual does not claim to address all of the safety issues associated with the us

12 Audit Trail80 XDLIB0712 Audit Trail12.1 IntroductionThe "audit trail" function electronically documents all operating steps carried out b

12 Audit TrailXDLIB07 81Fig. 12 - 2 Menu: Instrument settings/audit trailThe following window is shown. Log in with your user name and password:Fig. 1

12 Audit Trail82 XDLIB0712.2.2 Deactivating Audit TrailPress the "Menu" key to enter the main menu.Fig. 12 - 4 Main menuSelect "audit t

12 Audit TrailXDLIB07 8312.3 Audit Trail Main MenuTo enter the audit trail main menu, press the "Menu" key and select "audit trail"

12 Audit Trail84 XDLIB0712.5 Printing the Audit Trail Log FileIn the audit trail main menu, select "print audit trail".All documented operat

12 Audit TrailXDLIB07 854. In the audit trail main menu, select "export audit trail" and press "↵".The following display appears:F

12 Audit Trail86 XDLIB077. Click on "Receive". The log file is transferred to the PC.8. After exporting the file, "Export finished"

12 Audit TrailXDLIB07 87How to use "md5summer":1. Start "md5summer.exe".2. When asked "please select the root folder", s

12 Audit Trail88 XDLIB074. Select the md5 file which should be checked an press "Open".5. The check status and the result are displayed. A g

12 Audit TrailXDLIB07 89Fig. 12 - 10For the new log file, the entry "audit trail cleared" will automatically be created. This entry contains

2 Safety InstructionsXDLIB07 9• Follow the precautions below for the handling and measurement of inflammable samples and cleaning materials:- Do not s

12 Audit Trail90 XDLIB07Fig. 12 - 11 Menu: Audit trail/user management12.9.1 Adding a New UserSelect "add new user" to add new users (as man

12 Audit TrailXDLIB07 9112.9.3 Changing User SettingsSelect "change user settings".Select the user and press "↵".The same window a

12 Audit Trail92 XDLIB07Remove users yes (except himself/herself)no noPrint user settings yes no noHints:• Users with administrator or main user privi

Appendix A: Operation at High Air Humidity and/or Low Measuring TemperaturesXDLIB07 93Appendix A: Operation at High Air Humidity and/or Low Measuring

Appendix A: Operation at High Air Humidity and/or Low Measuring Temperatures94 XDLIB07For a measuring temperature of 20 °C, a drying cartridge must be

Appendix B: Technical DataXDLIB07 95Appendix B: Technical DataMeasuring range:0 to 3 g/cm3Repeatability, s. d.:Density:DMA 4500:DMA 5000:1 x 10-5 g/cm

Appendix B: Technical Data96 XDLIB07Important:All interfaces are designed to comply with SELV (Separated Extra-Low Voltage) requirements according to

Appendix B: Technical DataXDLIB07 97Printer interface (COM2): RS 232 C; 1200 to 9600 Baud; 1 or 2 stop bits; 7 or 8 data bits; no, odd or even parity;

Appendix C: Commands for Communication between PC and DMA 4500/500098 XDLIB07Appendix C: Commands for Communication between PC and DMA 4500/5000• Via

Appendix C: Commands for Communication between PC and DMA 4500/5000XDLIB07 99Interface cablePC-Serial Port(9-pin) RX232 RS2322...RXD 3...TXD4...DTR 5.